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Shanghai Jinghe Analytical Instrument Co., Ltd

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    shjhyq@163.com

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    13918032146/13818715366

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    C1 Production Base, 3rd Floor, No. 26 Lane 5018, Shangnan Road, Pudong New Area, Shanghai: Room 406, Building E, No. 245 Xinjun Ring Road, Pujiang Town, Minhang District, Shanghai

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AHS-G60 fully automatic headspace gas chromatograph

NegotiableUpdate on 01/21
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Overview

Brief description: The fully automatic headspace gas chromatograph has the advantages of high sample number, high heating number, fully automatic, compact structure, convenient human-machine interaction, and simple operation. The principle is to place the sample to be tested in a closed container, heat and raise the temperature to make the volatile components in the sample evaporate from the sample matrix. After reaching equilibrium, the upper gas is directly extracted and sent to post-processing equipment such as gas chromatography for analysis, thereby detecting the composition and content of volatile components in the sample.

Product Details

Main features of AnalyElf G60 gas chromatograph

Equipped with the fifth generation high-precision electronic circuit AFC/APC controller, with an accuracy of 0.001psi;

The retention time reproducibility is better than 0.05%, and the quantitative reproducibility is better than 0.5%;

The optimized injection port flow path is more reasonable, and the solvent peak is sharp without tailing;

Rich detector types, excellent performance, wide range FID detection limit better than 1.5pg/s;

Support dual tower sampling to improve analysis efficiency;

Personalized customized valve system allows you to easily face complex component analysis.


Fully automatic headspace gas chromatographperformance metrics

1. Temperature control range of headspace furnace: room temperature~260 ℃, step size 1 ℃

2. Temperature control range of valve injection system: room temperature~220 ℃, step size 1 ℃

3. Temperature control range of sample transfer pipeline: room temperature~220 ℃, step size 1 ℃

4. Temperature control accuracy:<± 0.1 ℃

5. Temperature control gradient:<± 0.1 ℃

6. Headspace furnace worker positions: 3 positions/6 positions/12 positions are optional

7. Headspace furnace oscillation mode: horizontal or vortex oscillation

8. Oscillation speed: fast, medium, and slow speed regulation

9. Headspace bottle workstation: 12 workstations/32 workstations/50 workstations are optional

10. Headspace bottle specifications: Standard 20ml, optional 10ml Headspace bottle plug-in

11. Injection pressure range: 0-0.4Mpa, continuously adjustable

12. Monitoring pressure range: 0-0.4Mpa, pressure gauge display

13. Analysis repeatability: RSD<1.5% (200ppm ethanol aqueous solution, related to GC performance)

14. Power supply: AC220V 50Hz

15. Power: 600W


Fully automatic headspace gas chromatographMain functions and features:

1. Fully automatic system, safe and reliable, one click operation, can be unattended

2. Modular design of software and hardware, compact structure

3. The software interface is rich in information, with simple human-computer interaction and easy operation. It has the following functions:

a) Display information includes: multi method parameter settings, real-time working status, running process and time information, etc

b) The headspace bottle, injection system, and sampling (injection) catheter are coordinated through software to achieve three-way heating and temperature control

c) 10 methods for editing, storing, and calling at any time

d) The GC and chromatographic data processing workstations can be synchronously started, and the device can also be started using external event programs to achieve multiple repeated injections of the same sample bottle

e) Equipped with self checking function (board level and gas circuit) and fault display function

4. Automatic positioning of the sample disk and real-time display of the disk number on the software end

5. The sample transfer tube (including sampling needle) and injection valve have automatic blowback function, which avoids cross contamination of different samples

6. The combination of a six way valve and a quantitative ring effectively reduces dead volume and improves analytical sensitivity

7. The six way valve and transmission pipeline link have no transmission cold points, ensuring the integrity of the sample

8. Support dual channel injection function for the same sample (user selectable)

9. Support sample bottle oscillation function, shorten balance time, improve sensitivity and repeatability


Application examples of headspace gas chromatography:Analysis of residual ethanol in blood

荆和谱图:血液乙醇分析专用柱1.png

pillar1BAC1)The spectrum above


荆和谱图:血液乙醇分析专用柱2.png

pillar2BAC2)The spectrum above

Injection method: Split injection+Split tube dual column system

Detector: 2 * FID

Peak order: 1. Ethanol; 2. Tert butanol (internal standard)

Applicability: Analysis of residual ethanol in blood


Standard curves for two analytical channelsAs shown in the following figure

FID1-柱1通道上的乙醇标准曲线.png


FID2-柱2通道上的乙醇标准曲线.png





A fully automatic headspace gas chromatograph is often interpreted as an instrument that combines a headspace sampler with a gas chromatograph. It is a chromatographic technique that adds a headspace injection device (divided into manual and automatic) in front of the gas chromatograph injection port. It has minimal harm to analysts and the environment, is easy to operate, has good reproducibility, and accurate injection volume. It is an analytical method that meets the requirements of "green analytical chemistry" and has the following advantages over ordinary chromatographic analysis:
1. Wide applicability
Headspace gas chromatography can analyze both volatile components in liquid samples and volatile substances in solid samples; It can analyze single component volatile gas samples or separate and analyze complex volatile component mixtures; It can be used for both constant headspace gas sample analysis and detection of low levels of volatile components.
2. Fast and accurate injection
Directly take volatile gaseous samples of liquid samples (or solid samples) and send them to the gas chromatograph for separation and analysis. In many cases, sample pretreatment operations can be eliminated and there are fewer human interference factors, making this method faster and simpler than ordinary chromatographic analysis. In addition, due to the use of quantitative tube injection, the analysis is more accurate.
3. High sensitivity and good reproducibility
Sometimes lower detection limits can be obtained than ordinary gas chromatography analysis, because it avoids solvent interference caused by conventional sample pretreatment processes and certain peculiarities of headspace samples. For liquid or solid samples that are easy to decompose and cannot be directly analyzed by injection, they have more practical value. Its pressure balance is automatically injected, with better reproducibility.