Shanghai PTC-III Solid/Liquid Blow and Capture Instrument

Instrument Introduction:

The PTC-III solid/liquid blow and capture instrument is a 70 position solid-liquid integrated fully automatic blow and capture instrument with an electronic cold trap. Liquid samples can be automatically and accurately sampled into blowing bottles for blowing and capturing, or solid samples can be automatically added to distilled water and shaken for direct blowing and capturing. By combining with GC or GC/MS, it can be widely applied in environmental analysis, such as the analysis of organic pollutants in drinking water, wastewater, and soil, as well as the analysis of volatile compounds (such as odor components) in food. This instrument complies with standards such as "HJ639-2012 Determination of Volatile Organic Compounds in Water Quality by Sweep Capture/Gas Chromatography Mass Spectrometry", "HJ686-2014 Determination of Volatile Organic Compounds in Water Quality by Sweep Capture/Gas Chromatography Mass Spectrometry", and "HJ605-2011 Determination of Volatile Organic Compounds in Soil and Sediments by Sweep Capture/Gas Chromatography Mass Spectrometry".

working conditions

Power supply: 220VAC ± 22VAC 50Hz ± 0.5Hz

Backblowing carrier gas pressure: ≤ 0.4MPa

Environmental temperature: 5-35 ℃

Relative humidity: ≤ 85%

Technical Specifications:

Sample grade: 70, 40ml VOA sample bottle

Purging tube temperature: room temperature~100 ℃, control accuracy ± 1 ℃

Cold trap (electronic semiconductor refrigeration) temperature: Z low cooling temperature can reach minus 30 degrees Celsius

Capture tube desorption temperature: 150-380 ℃, heating rate>2400 ℃/min; Reduce from 250 ℃ to 35 ℃ within 90 seconds

Heating temperature of pipeline: 50-220 ℃, control accuracy ± 1 ℃

Heating temperature of water purifier: room temperature~400 ℃

Cleaning distilled water temperature: room temperature~90 ℃, control accuracy ± 1 ℃

Solid sample bottle heating: room temperature~100 ℃, control accuracy ± 1 ℃

Solid sample mixing: 5ml distilled water, shake and mix

Glass blowing tube: 5ml blowing tube

Capture trap size: stainless steel material Φ 3mm × 180mm × 0.1mm

Blow flow rate: 10-150ml/minute

Z high power:<800VA

Timing range: 1 second to 99 minutes and 59 seconds

Timing error:<0.1%

Gas path pressure resistance:>0.4MPa

Synchronous signal output: Two 1-2 second switching signals

Instrument dimensions: height * width * length 620mm * 840mm * 450mm

Weight: Approximately 40Kg

Key Features:

Strong universal performance: can be used in combination with any brand of gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS);

Easy to operate, convenient to use, fully controlled by software, high degree of automation: simply place the sample tube into the sample tray, and all operations and controls are completed by the control software, resulting in good sample repeatability; The large touch LCD panel design in the host can track temperature and operation commands throughout the process.

The cold trap adopts semiconductor refrigeration+air cooling, with a low cooling temperature of up to -30 ℃ (at room temperature of 20 ℃), meeting most low-temperature enrichment needs.

The trap is heated using direct resistance heating, with a heating rate greater than 2400 ℃/min.

The built-in foam sensor can detect the foam in the purging pipe to prevent the way of polluting the sample and protect the entire analysis system.

Users can customize the cleaning frequency of the sampling needle and blowing tube.

Solid sample bottles can be heated and directly injected with distilled water for shaking, mixing, and blowing.

Capture trap and blowback tube for gas separation to reduce cross contamination between samples. In the blowback cycle, the compounds blown out from the trap will not flow into the purge tube.

The water trap removes water vapor at the blowing end, greatly reducing the impact of water vapor on GC and GC/MS.

The sample tubing is made of PEEK material and treated with silane inert stainless steel to reduce residual pollution.

Hot water can be used to flush and blow pipes to reduce residue.

All pipelines and six way valves are temperature controlled for heating, eliminating system cold spots and reducing sample loss.

Provide a synchronization interface that allows for simultaneous activation of chromatography and workstation during sample injection