Synchronous Thermal Analyzer (STA 449 F3 Jupiter)

1、 Instrument Introduction:

STA 449 F3 Jupiter ®It is a newly launched synchronous device by NikeTG-DSCThermal analyzer. As a cost-effective optionNETZSCH F3One of the new members of the product series, It has the characteristics of being sturdy, flexible, and easy to operate, making it very suitable for testing both thermal effects (transition temperature, enthalpy) and changes in mass simultaneously. By selecting the appropriate furnace body, installing high-performance sensors, and matching them with the most appropriate accessories, adopting a synchronous thermal analyzer with top mounted samples can almost meet all applications. It combines high-performance heat flow typeDSCCompared to high-sensitivity scales, it can provide unparalleled weighing and measurement range.

STA 449 F3 Jupiter ®Contains high-performance componentsTGgiveDSCTesting system. Its balance system has the characteristics of small drift and wide range. This system can be equipped with scales of different ranges and achieve high sensitivity across the entire range. This is attributed to Ling's advanced electronic balance technology.

As a renowned figure of NikeSTA 449 CThe replacement product,STA 449 F3 Jupiter ®Fully inheritedSTA 449 Cof“Broad mind”According to different furnace bodies, the temperature range of this system can reach -150℃… 2400℃.

Through the vacuum system and flow control system, users can conduct tests under any atmosphere control.

Double furnace lifting device and automatic sampler（ASC）It is very advantageous for high-performance thermal analysis instruments, which can greatly improve the sample processing capacity and thus enhance the efficiency of testing.

Within a wide temperature range, variousTG-DSCSensors can provide trueDSCTesting.TG、TG-DTASensors can meet special testing requirements.

Durable and sturdy hardware, user-friendly software, flexible and diverse designs, coupled with a wide range of options, makeSTA 449 F3Be the ideal tool for quality control and material research in your laboratory.

STA 449 F3 Jupiter ®Can be withQMSorFTIRIt can also be used in combination with both. Even with an automatic sampler, all tests can be conducted synchronously.

2、 Technical parameters:

●Temperature range:-150 . .. 2400℃

●Heating and cooling rate:0.001 . .. 50 K/min(Depending on the furnace configuration; high-speed heating furnace has the highest linear heating rate)1000 K/min）

●Zui Large Scale Weight:35000 mg

●Weighing resolution:0.1 μg(Within the full range)

●DSCResolution:< 1μW(depending on the equipped sensors)

●Atmosphere: Inert, Oxidation, Reduction, Static, Dynamic

●Standard configuration for 2 Road blowing and sweeping air 1 Electromagnetic valve for road protection gas.

●3 Mass flow meter for road gas, used for digital precise control of gas flow rate (optional)

●Vacuum sealed structure, vacuum degree10-4 mbar

●For singleTGBracket can be equipped withc-DTA ®(Computational type)DTA）Function, used for temperature correction and additionalDTAInformation acquisition.

●TG-DSCgiveTG-DTASample holder, used for true synchronous measurement.

●Automatic sampler（ASC）, Zui Duo can be loaded simultaneously 20 Sample (optional)

●Through a heatable adapter andFTIR，MSas well asGC-MSCombination (optional)

●uniquePulse-TA ®Extended functions (optional)

●uniqueOTS ®Oxygen inhalation accessories (optional)

3、 Software functions:

TA 449 F3 Jupiter ® -FUNCTION

STA 449 F3 Jupiter ®The measurement and analysis software is based onMicroSoft Windows ®systemicProteus ®The software package includes all necessary measurement and data analysis functions. This software package has an extremely user-friendly interface, including easy to understand menu operations and automated workflows, and is suitable for various complex analyses.ProteusThe software can be installed on the control computer of the instrument to work online, or installed on other computers for offline use.

DSC/DTAPartial analysis functions:

●Peak annotation: It can determine the starting point, peak value, inflection point, and ending point temperature, and can perform automatic peak search.

●peak area/Enthalpy calculation: Multiple types of baselines can be selected for partial area analysis. You can choose the current mass at which temperature to use as the benchmark for enthalpy calculation.

●Comprehensive analysis of peaks: Various information such as temperature, area, peak height, and peak width can be obtained simultaneously in one annotation.

●Comprehensive glass transition analysis.

●Automatic baseline deduction.

●Crystallinity calculation.

●Oxidation induction period（O.I.T.）Analysis.

●Specific heat analysis (optional).

●BeFlat ®Function: Used forDSCOptimization of baseline (optional).

●Tau-R ®mode:Incorporate the time constant and thermal resistance of the instrument into the calculation,To obtain sharperDSCPeak shape（DSCSensor optional function

●DSCPeak shape correction function: Correct the peak shape of the absorption/release peaks, incorporating the thermal resistance and time constant factors of the system into the calculation (optional).

TGPartial analysis functions:

●Manual or automatic annotation of weightlessness steps, units%perhapsmg.

●quality-time/Temperature labeling.

●Residual quality labeling.

●The extrapolation starting and ending points of the weightlessness step can be marked.

●Can perform first-order differentiation on the thermogravimetric curve（DTG）It can be differentiated with second-order differentiation and labeled with peak temperature.

●Automatic baseline and buoyancy effect correction.

●c-DTA ®(Computational type)DTA）: Can annotate thermal effect characteristic temperature and peak area (optional)

Related advanced software:

●Peak Separation Software

●Dynamics software

4、 Related attachments

STA 449 F3We provide crucibles made of various materials such as alumina, platinum, aluminum, graphite, quartz, etc. Multiple different size specifications are provided for each crucible.

A unique steam stove option, equipped with a series of accessories for steam generation, gas mixing, and flow control, constitutes the highest possible humidity under the set conditions 1250℃A tool for studying the changes in mass and energy inside a sample within a temperature range.

The newly launched high-speed furnace body is a modification of the existing oneSTAWith high temperatureDSCA great feature extension for the product. This type of furnace body does not need to be equipped with specialized instruments and can be installed together with other furnace bodies in existing onesSTA449F / DSC404FOn the double lifting device. If dual furnace bodies are not installed, an automatic sampler can also be equipped for the high-speed furnace（ASC）. The flexibility of this modular design, especially the high-speed furnace canASCCombined, it saves a lot of time and greatly shortens the sampling cycle.

For samples that are prone to oxidation at high temperatures, they can be equipped withOTS ™（Oxygen Trap System）Attachment: Absorb and purge impurity oxygen in the atmosphere, effectively reducing the possibility of sample oxidation.

Automatic sampling system（ASC）Can be used for batch routine testing. The instrument can work day and night, not only making full use of the instrument but also saving a lot of time. (For example, conducting calibration tests on weekends when there is no one present). The injection turntable can be placed at most once 20 Sample and reference crucible, and work in a customized order. The testing atmosphere and cooling device control are both automatic. Individual test condition programming and macro calculations can be performed for each sample. An easy to understand operating interface can guide users to complete a series of test program edits, and during the experiment, they can also make changes to the running program by inserting new test programs into the already written program.