Synchronous Thermal Analyzer (STA 449 F1 Jupiter)

1、 Instrument Introduction:

STA 449 F1 Jupiter ® It is an advanced synchronous TG-DSC analytical instrument newly launched by Nike, which has unlimited configuration flexibility and unparalleled excellent performance.

●cover -150 to 2400℃ A wide temperature range.

●It can quickly and deeply characterize the thermal stability, decomposition behavior, component analysis, phase transition, melting process, etc. of materials.

●Easy to use top mounted style system, weighing system with extremely high resolution (25ng resolution, weighing range 5g), and high long-term stability.

●A freely replaceable DSC sensor with extremely high sensitivity and repeatability, used for measuring reaction/transition temperature and enthalpy, as well as specific heat.

●A large number of optional enhancement accessories to meet the diverse and extensive needs of customers.

●The furnace body can be equipped with multiple different temperature ranges and performance indicators simultaneously, which can be switched by users themselves. (For a dual furnace structure, a rotating dual lifting device can be installed as an option)

●Pluggable sample holder（TG，TG-DSC，TG-DTAEtc.)

●Zui Duo can be loaded simultaneously 20 An automatic sampler for a sample（ASC）

●Automatic vacuum pumping and filling device（Autovac）

●A large number of accessories are available for selection, such as sample crucibles with various materials, shapes, and sizes to choose from.

●STAUnique temperature modulationDSC（TM-DSC）

●Provide additional interfaces andMS、FTIRConnecting can enable even more complex analysis.

Nike STA 449 F1 Jupiter ® It can simultaneously test thermal effects (transition temperature, enthalpy) and changes in mass, with excellent stability, resolution, and accuracy. By selecting the appropriate furnace body, installing high-performance sensors, and matching them with appropriate accessories, a synchronous thermal analyzer with top mounted samples can almost meet all applications. It combines high-performance thermal flow DSC with advanced nanogram scale balance, ensuring bothDSCThe high sensitivity and resolution of the test ensureTGHigh resolution, low noise, and drift stability for testing.

STA 449 F1 Jupiter ®Integrated with the newly launchedTGSystem andDSCSystem, its high temperatureDSCCan test the specific heat of samples within the ultra-high temperature range. The temperature range of the entire system is-150℃…2000℃(depending on the specific furnace body and sensor configuration). Double furnace lifting device and automatic sampler（ASC）Greatly improved the sample processing capacity,ASCIt can be automatically tested at night or on weekends. variousDSCThe sensor provides a wide temperature range（-150℃…1750℃）The real oneDSCTesting can accurately measure small phase transitions and specific heat values.

The vacuum sealed design and high-resolution, metal encapsulated mass flow controller make the entire system a popular choice in research and industrial fieldsTGandDSCThe ideal tool for testing.

This fully equipped thermal analysis system can easily analyze trace amounts of active new drugs, trace impurities on semiconductor waveform converters, electronic components, medical transplants, and deviations in inorganic mixture components. Use ourSTA 449 F1 Jupiter ®You will have an extraordinary feeling.

For the analysis of escaping gases,STACan be withQMSorFTIRIt can also be used in combination with both. Even with an automatic sampler, all tests can be conducted synchronously.

IISTA 449 F1 Jupiter ® -Technical parameters:

●Temperature range:-150 . .. 2400℃

●Heating and cooling rate:0.001 . .. 50 K/min(Depending on the furnace configuration; high-speed heating furnace has the highest linear heating rate)1000 K/min）

●Weighing range:5000 mg

●TGResolution:0.025 μg

●DSCResolution:< 1 μW(depending on the equipped sensors)

●Atmosphere: Inert, Oxidation, Reduction, Static, Dynamic, Vacuum

●Integrated quality flow meter with 2 Road blowing and sweeping air 1 Road protection gas

●High vacuum structure design, with a vacuum degree of up to10-4 mbar（10-2 pa）

●For singleTGBracket can be equipped withc-DTA ®(Computational type)DTA）Function, used for temperature correction and additionalDTAInformation acquisition.

●TG-DSCgiveTG-DTASample holder, used for true synchronous measurement.

●Automatic sampler（ASC）, Zui Duo can be loaded simultaneously 20 Sample (optional)

●Through a heatable adapter andFTIR，MSas well asGC-MSCombination (optional)

●uniquePulse-TAExtended functions (optional)

IIISTA 449 F1 Jupiter ® -FUNCTION

STA 449 F1 Jupiter ®The analysis and operation software is based onMS ® Windows ® XPgiveVista ®systemicProteus ®The software package includes all necessary measurement and data analysis functions. This software package has an extremely user-friendly interface, including easy to understand menu operations and automated workflows, and is suitable for various complex analyses.ProteusThe software can be installed on the control computer of the instrument to work online, or installed on other computers for offline use.

DSC/DTAPartial analysis functions:

●Peak annotation: It can determine the starting point, peak value, inflection point, and ending point temperature, and can perform automatic peak search.

●peak area/Enthalpy calculation: Multiple types of baselines can be selected for partial area analysis. You can choose the current mass at which temperature to use as the benchmark for enthalpy calculation.

●Comprehensive analysis of peaks: Various information such as temperature, area, peak height, and peak width can be obtained simultaneously in one annotation.

●Comprehensive glass transition analysis.

●Automatic baseline deduction.

●Crystallinity calculation.

●Oxidation induction period（O.I.T.）Analysis.

●Specific heat analysis (optional).

●BeFlat ®Function: Used forDSCOptimization of baseline (optional).

●DSCPeak shape correction function: Correct the peak shape of the absorption/release peaks, incorporating the thermal resistance and time constant factors of the system into the calculation (optional).

●TM-DSC(Optional).

TGPartial analysis functions:

●Manual or automatic annotation of weightlessness steps, units%perhapsmg.

●quality-time/Temperature labeling.

●Residual quality labeling.

●The extrapolation starting and ending points of the weightlessness step can be marked.

●Can perform first-order differentiation on the thermogravimetric curve（DTG）It can be differentiated with second-order differentiation and labeled with peak temperature.

●Automatic baseline and buoyancy effect correction.

●c-DTA ®(Computational type)DTA）: Can annotate thermal effect characteristic temperature and peak area (optional)

Related advanced software:

●Peak Separation Software

●Dynamics software

4STA 449 F1 Jupiter ® -Related attachments:

Wide crucible selection:NETZSCHWe provide various crucibles such as aluminum, silver, gold, copper, platinum, alumina, zirconia, graphite, stainless steel, etc., which can meet almost all material testing and applications.

A unique steam stove option, equipped with a series of accessories for steam generation, gas mixing, and flow control, constitutes the highest possible humidity under the set conditions 1250℃A tool for studying the changes in mass and energy inside a sample within a temperature range.

If testing is required in a special atmosphere,STA 449 F1 Jupiter ®Special anti-corrosion configurations can be provided. This configuration can be tested in corrosive or reducing atmospheres, with the gas flow control system placed in a separate box, the sample holder also specially configured, and the thermocouple in a protected state.

For very special samples or radioactive materials,STA 449 F1 Jupiter ®It can be installed in glove boxes or hot chambers, with electronic components located away from the measuring unit, and all data cables and supporting equipment can be connected to one lead.

The newly launched high-speed furnace body is a modification of the existing oneSTAWith high temperatureDSCA great feature extension for the product. This type of furnace body does not need to be equipped with specialized instruments and can be installed together with other furnace bodies in existing onesSTA449F / DSC404FOn the double lifting device. If dual furnace bodies are not installed, an automatic sampler can also be equipped for the high-speed furnace（ASC）. The flexibility of this modular design, especially the high-speed furnace canASCCombined, it saves a lot of time and greatly shortens the sampling cycle.

For samples that are prone to oxidation at high temperatures, they can be equipped withOTS ™（Oxygen Trap System）Attachment: Absorb and purge impurity oxygen in the atmosphere, effectively reducing the possibility of sample oxidation.

Automatic sampling system（ASC）Can be used for batch routine testing. The instrument can work day and night, not only making full use of the instrument but also saving a lot of time. (For example, conducting calibration tests on weekends when there is no one present). The injection turntable can be placed at most once 20 Sample and reference crucible, and work in a customized order. The testing atmosphere and cooling device control are both automatic. Individual test condition programming and macro calculations can be performed for each sample. An easy to understand operating interface can guide users to complete a series of test program edits, and during the experiment, they can also make changes to the running program by inserting new test programs into the already written program.